IUPAC-NIST Solubility Database
NIST Standard Reference Database 106

Glass Ball as Bullet Solubility System: 1-Bromo-3-chloropropane with Water

   (1) Water; H2O; [7732-18-5]  NIST Chemistry WebBook for detail
   (2) 1-Bromo-3-chloropropane; C3H6BrCl; [109-70-6]  NIST Chemistry WebBook for detail

Original Measurements:
   Miller, M.M.; Wasik, S.P.; Huang, G.L.; Shiu, W.Y.; Mackay, D., Environ. Sci. Technol. 1985, 19, 522-529.

   Temperature = 298 K

Prepared By:
   A. L. Horvath

Experimental Data:   (Notes on the Nomenclature)
t/°C102 * Mass Fraction w1 (compiler) 104 * Mole Fraction x1 (compiler)n1/V2 [mol m**-3]
250.2242.561.42 x 101
   A saturated aqueous solution was prepared by passing of water through a column which was packed with glass beads coated with 1-bromo-3-chloropropane. The saturated solution was then pumped through an  extractor column and 1-bromo-3-chloropropane was extracted directly into an analytical column. The samples were analyzed with a liquid chromatograph equipped with both an UV absorbance and a  fluorescence detector with excitation filters. The peak area was established using a Hewlett-Packard recorder.

Source and Purity of Materials:
   (1) Eastman Kodak Company, commercial quality, used as received.
   (2) Double distilled.

Estimated Errors:
   Solubility: Not specified.
   Temperature: ± 0.5 K (compiler).