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IUPAC-NIST Solubility Database
NIST Standard Reference Database 106
Solubility System:
1,3-Dibromopropane with Water
Components:
(1) Water; H2O; [7732-18-5]
NIST Chemistry WebBook
for detail
(2) 1,3-Dibromopropane; C3H6Br2; [109-64-8]
NIST Chemistry WebBook
for detail
Original Measurements:
Gross, P.M.; Saylor, J.H.; Gorman, M.A., J. Am. Chem. Soc. 1933, 55(2), 650-2.
Variables:
Temperature = 303 K
Prepared By:
A. L. Horvath
Experimental Data:
(Notes on the Nomenclature)
t/°C
10
3
* g
1
/g
2
10
2
* Mass Fraction w
1
(compiler)
10
4
* Mole Fraction x
1
(compiler)
30
1.68
0.168
1.50
Method/Apparatus/Procedure:
The saturated solution was prepared in a flask and placed in a waterbath thermostat. The samples were analyzed using a Zeiss combination liquid and gas interferometer described elsewhere.
1
A detailed description of the complete procedure is given in a M. A. thesis.
2
Source and Purity of Materials:
(1) Eastman Kodak Company, fractionally distilled before use. The b. p. range was 166.64 - 166.86°C.
(2) Distilled.
Estimated Errors:
Solubility: ± 0.5 %.
Temperature: ± 0.02 K.
References:
1
P. M. Gross and J. H. Saylor, J. Am. Chem. Soc. 53, 1744 (1931).
2
M. A. Gorman, MA thesis, Duke University, Durham, 1932.