IUPAC-NIST Solubility Database
NIST Standard Reference Database 106

Glass Ball as Bullet Solubility System: 1,3-Dichloropropane with Water
Components:
   (1) Water; H2O; [7732-18-5]  NIST Chemistry WebBook for detail
   (2) 1,3-Dichloropropane; C3H6Cl2; [142-28-9]  NIST Chemistry WebBook for detail
Original Measurements:
   Gross, P.M.; Saylor, J.H.; Gorman, M.A., J. Am. Chem. Soc. 1933, 55(2), 650-2.

 Variables:
   Temperature = 298 K

 Prepared By:
   A. L. Horvath

 Experimental Data:   (Notes on the Nomenclature)
  
t/°C103 * g1/g2102 * Mass Fraction w1 (compiler) 104 * Mole Fraction x1 (compiler)
302.870.2864.57
 Method/Apparatus/Procedure:
   The saturated solution was prepared in a flask and placed in a waterbath thermostat. The samples were analyzed using a Zeiss combination liquid and gas interferometer  described elsewhere.1 A detailed description of the complete procedure is given in a M. A. thesis.2

 Source and Purity of Materials:
   (1) Eastman Kodak Company, distilled fractionally before use. The b. p. range was 120.5 - 120.6°C.
   (2) Distilled.

 Estimated Errors:
   Solubility: ± 1.0 %.
   Temperature: ± 0.02 K.

 References:
   1 P. M. Gross and J. H. Saylor, J. Am. Chem. Soc. 53, 1744 (1931).
   2 M. A. Gorman, MA thesis, Duke University, Durham, 1932.