IUPAC-NIST Solubility Database
NIST Standard Reference Database 106

Glass Ball as Bullet Solubility System: 1-Iodopropane with Water
Components:
   (1) Water; H2O; [7732-18-5]  NIST Chemistry WebBook for detail
   (2) 1-Iodopropane; C3H7I; [107-08-4]  NIST Chemistry WebBook for detail
Original Measurements:
   Gross, P.M.; Saylor, J.H., J. Am. Chem. Soc. 1931, 53, 1744-51.

 Variables:
   Temperature = 303 K

 Prepared By:
   A. L. Horvath

 Experimental Data:   (Notes on the Nomenclature)
  
t/°C103 * g1/g2102 * Mass Fraction w1 (compiler) 104 * Mole Fraction x1 (compiler)
301.040.1041.10
 Method/Apparatus/Procedure:
   An excess of 1-iodopropane in 500 g water was shaken for 12 hours in a waterbath thermostat. Samples were then withdrawn and read against pure water in an interferometer made by Zeiss.1 A detailed description of the  complete procedure is given in a Ph. D. thesis.2

 Source and Purity of Materials:
   (1) Eastman Kodak Company, shaken with Na2S2O3 solution and distilled water, and fractionated before use.
   (2) Distilled.

 Estimated Errors:
   Solubility: ± 3.0 %.
   Temperature: ± 0.02 K.

 References:
   1 P. M. Gross, J. Am. Chem. Soc. 51, 2362 (1929).
   2 J. H. Saylor, Ph.D. thesis, Duke University, Durham, 1930.