IUPAC-NIST Solubility Database
NIST Standard Reference Database 106

Glass Ball as Bullet Solubility System: Nitromethane with 1,2-Ethanediol-d2
Components:
   (1) Nitromethane; CH3NO2; [75-52-5]  NIST Chemistry WebBook for detail
   (2) 1,2-Ethanediol-d2; C2D2H4O2; [7782-39-0]  NIST Chemistry WebBook for detail
Original Measurements:
   Tsvetkov, V.G.; Rabinovich, I.B., Zh. Fiz. Khim. 47, 2403 (1973).

 Variables:
   Temperature = 321 K

 Prepared By:
   V. P. Sazonov

 Experimental Remarks:
   The upper critical solution temperature was reported to be 47.5 °C (320.7 K, compiler).

 Experimental Data:   (Notes on the Nomenclature)
   Method/Apparatus/Procedure:
   The synthetic method1 was used. No further details were reported.

 Source and Purity of Materials:
   (1) Source not specified; purity not specified; purified.
   (2) Obtained by method described in Ref. 1. The O.D. group of the product had a deuterium content of 97 at. %.

 Estimated Errors:

   Temperature: ± 0.1 K.

 References:
   1 A. V. Nikolaev, Yu. A. Dyadin, and I. I. Yakovlev, Dokl. Akad. Nauk SSSR 170, 110 (1966).