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IUPAC-NIST Solubility Database
NIST Standard Reference Database 106
Solubility System:
Nitromethane with Cyclohexanol
Components:
(1) Nitromethane; CH3NO2; [75-52-5]
NIST Chemistry WebBook
for detail
(2) Cyclohexanol; C6H12O; [108-93-0]
NIST Chemistry WebBook
for detail
Original Measurements:
Erofeeva, L.F.; Yunnikova, N.V., Sb. Nauch. Tr., Kuzbas. Polytekh. Inst. 26, 1-6 (1971).
Variables:
Temperature = 275 K to 291 K
Prepared By:
V. P. Sazonov
Experimental Data:
(Notes on the Nomenclature)
Mutual solubility of nitromethane and cyclohexanol
t/°C
T/K
Mass Fraction w
1
(compiler)
Mole Fraction x
1
(compiler)
Comment(s)
1.8
275.0
- x 10
2
-
Alcohol-rich phase
1.8
275.0
87.5 x 10
2
0.920
Nitromethane-rich phase
2.3
275.5
30.8 x 10
2
0.422
Alcohol-rich phase
2.3
275.5
- x 10
2
-
Nitromethane-rich phase
4.2
277.4
33.3 x 10
2
0.450
Alcohol-rich phase
4.2
277.4
- x 10
2
-
Nitromethane-rich phase
6.3
279.5
35.9 x 10
2
0.479
Alcohol-rich phase
6.3
279.5
85.0 x 10
2
0.903
Nitromethane-rich phase
8.6
281.8
39.2 x 10
2
0.514
Alcohol-rich phase
8.6
281.8
- x 10
2
-
Nitromethane-rich phase
8.7
281.9
- x 10
2
-
Alcohol-rich phase
8.7
281.9
84.0 x 10
2
0.896
Nitromethane-rich phase
12.0
285.2
45.2 x 10
2
0.575
Alcohol-rich phase
12.0
285.2
- x 10
2
-
Nitromethane-rich phase
13.8
287.0
49.2 x 10
2
0.614
Alcohol-rich phase
13.8
287.0
- x 10
2
-
Nitromethane-rich phase
14.9
288.1
51.4 x 10
2
0.634
Alcohol-rich phase
14.9
288.1
- x 10
2
-
Nitromethane-rich phase
15.4
288.6
- x 10
2
-
Alcohol-rich phase
15.4
288.6
75.9 x 10
2
0.838
Nitromethane-rich phase
15.6
288.8
54.6 x 10
2
0.664
Alcohol-rich phase
15.6
288.8
- x 10
2
-
Nitromethane-rich phase
16.5
289.7
59.2 x 10
2
0.704
Alcohol-rich phase
16.5
289.7
- x 10
2
-
Nitromethane-rich phase
16.8
290.0
- x 10
2
-
Alcohol-rich phase
16.8
290.0
71.3 x 10
2
0.803
Nitromethane-rich phase
16.9
290.1
62.9 x 10
2
0.736
Alcohol-rich phase
16.9
290.1
- x 10
2
-
Nitromethane-rich phase
16.9
290.1
65.7 x 10
2
0.759
Alcohol-rich phase
16.9
290.1
- x 10
2
-
Nitromethane-rich phase
17.5
290.7
66.0 x 10
2
0.761
Alcohol-rich phase
17.5
290.7
66.0 x 10
2
0.761 (UCST)
Nitromethane-rich phase
Method/Apparatus/Procedure:
The synthetic method
1
was used. No further details were reported.
Source and Purity of Materials:
(1) Source not specified; pure grade reagent; distilled.
(2) Source not specified; pure grade reagent; dried and distilled under vacuum.
Estimated Errors:
Solubility: Not reported.
Temperature: Not reported.
Pressure: Not reported.
References:
1
V. F. Alekseev, Zh. Russ. Fiz.-Khim. O-va 8, 249 (1876).