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IUPAC-NIST Solubility Database
NIST Standard Reference Database 106
Solubility System:
Nitromethane with 1-Decanol
Components:
(1) Nitromethane; CH3NO2; [75-52-5]
NIST Chemistry WebBook
for detail
(2) 1-Decanol; C10H22O; [112-30-1]
NIST Chemistry WebBook
for detail
Original Measurements:
Zhuravleva, I.K.; Zhuravlev, E.F.; Lomakina, N.G., Zh. Fiz. Khim. 51, 1700-7 (1977).
Variables:
Temperature = 301 K to 331 K
Prepared By:
V. P. Sazonov
Experimental Data:
(Notes on the Nomenclature)
Mutual solubility of nitromethane and 1-decanol
t/°C
T/K
10
2
* Mass Fraction w
1
Mole Fraction x
1
(compiler)
Comment(s)
27.5
300.7
10.0
0.224
Hydrocarbon-rich phase
27.5
300.7
-
-
Nitromethane-rich phase
41.0
314.2
-
-
Hydrocarbon-rich phase
41.0
314.2
90.0
0.959
Nitromethane-rich phase
46.5
319.7
20.0
0.393
Hydrocarbon-rich phase
46.5
319.7
-
-
Nitromethane-rich phase
53.0
326.2
-
-
Hydrocarbon-rich phase
53.0
326.2
80.0
0.912
Nitromethane-rich phase
53.5
326.7
30.0
0.526
Hydrocarbon-rich phase
53.5
326.7
-
-
Nitromethane-rich phase
56.5
329.7
40.0
0.633
Hydrocarbon-rich phase
56.5
329.7
-
-
Nitromethane-rich phase
57.0
330.2
50.0
0.722
Hydrocarbon-rich phase
57.0
330.2
70.0
0.858
Nitromethane-rich phase
58.0
331.2
-
-
Hydrocarbon-rich phase
58.0
331.2
60.0
0.796
Nitromethane-rich phase
57.5
330.7
-
-
Hydrocarbon-rich phase
57.5
330.7
-
- (UCST)
Nitromethane-rich phase
Method/Apparatus/Procedure:
The synthetic method
1
was used. No further details were reported.
Source and Purity of Materials:
(1) Source not specificed, purity not specified;
n
(20 °C, D) = 1.3820,
d
(20 °C) = 1133.0 g·L
-1
.
a
(2) Source not specified; purified not specified;
n
(20 °C, D) = 1.4370,
d
(20 °C) = 830 g·L
-1
.
a
Recorded as 1330.0 in original. Value corrected by compiler.
Estimated Errors:
Solubility: Not reported.
Temperature: Not reported.
Pressure: Not reported.
References:
1
V. F. Alekseev, Zh. Russ. Fiz.-Khim. O-va 8, 249 (1876).