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IUPAC-NIST Solubility Database
NIST Standard Reference Database 106
Solubility System:
Nitromethane with N, N-Diethylethanamine
Components:
(1) Nitromethane; CH3NO2; [75-52-5]
NIST Chemistry WebBook
for detail
(2) N,N-Diethylethanamine; C6H15N; [121-44-8]
NIST Chemistry WebBook
for detail
Original Measurements:
Zhuravlev, E.F.; Burdykina, P.I., Zh. Fiz. Khim. 43, 895-900 (1969).
Variables:
Temperature = 273 K and 285 K
Prepared By:
V. P. Sazonov
Experimental Data:
(Notes on the Nomenclature)
Mutual solubility of nitromethane and N,N-diethylethanamine
t/°C
T/K
10
2
* Mass Fraction w
1
Mole Fraction x
1
(compiler)
Comment(s)
0.0
273.2
22.4
0.324
Amine-rich phase
0.0
273.2
74.8
0.831
Nitromethane-rich phase
11.6
284.8
53.5
0.656
Amine-rich phase
11.6
284.8
53.5
0.656 (UCST)
Nitromethane-rich phase
Method/Apparatus/Procedure:
The synthetic method
1
was used. No further details were reported.
Source and Purity of Materials:
(1) Source not specified; purity not specified; distilled.
(2) Source not specified; purity not specified; distilled.
Estimated Errors:
Solubility: Not reported.
Temperature: Not reported.
Pressure: Not reported.
References:
1
V. F. Alekseev, Zh. Russ. Fiz.-Khim. O-va 8, 249 (1876).