IUPAC-NIST Solubility Database
NIST Standard Reference Database 106


Glass Ball as Bullet Solubility System: Nitroethane with oil fraction of Tuimazin crude

Components:
   (1) Nitroethane; C2H5NO2; [79-24-3]  NIST Chemistry WebBook for detail
   (2) Oil fraction of Tuimazin crude; ; []  NIST Chemistry WebBook for detail

Original Measurements:
   Pol’shinskii, V.V.; Kozlov, L.M., Khim. Tekhnol. Topl. Masel (10), 9-13 (1970).

Variables:
   Temperature = 279 K to 377 K

Prepared By:
   V. P. Sazonov and N. I. Lisov

Experimental Remarks:

   Values of critical solution temperatures of nitroethane (1) and stocks of fractions of Tuimazin crude (2) are presented over the temperature range in graphical form.

Experimental Data:   (Notes on the Nomenclature)
  
Mean values of critical solution temperatures of nitroethane (1) and stocks of oil fraction of Tuimazin crude (2)
t/°CT/KChemical NameDensity ρ [20 °C,4 °C]n1/V2 [20 °C,D]
6279Heavily aromatics1.0232-1.04791.5787-1.5979
30303Mean aromatics0.9706-0.99211.5430-1.5623
64337Light aromatics0.91761.5090
104377Paraffin-naphthenes0.8195-0.86671.420*-1.4756
Notes:
   *  n(70 °C,D)

Method/Apparatus/Procedure:
   The method, described in Bondarev and Kozlov,1 was used. No experimental details given.

Source and Purity of Materials:
   (1) Source not specified; purity not specified; purified; n(20°C,D) = 1.3919; d(20°C, 4°C) = 1.0596.
   (2) Obtained by distillation of Tuimazin crude between 440 and 520°C; stocks obtained by division of oil fraction on silica gel by liquid chromatography.

Estimated Errors:
   Solubility: Not specified.
   Temperature: Not specified.

References:
   1 S. V. Bondarev and L. M. Kozlov, Khim. Tekhnol. Topl. Masel (10), 10 (1968).