IUPAC-NIST Solubility Database
NIST Standard Reference Database 106

Glass Ball as Bullet Solubility System: Nitroethane with Water
Components:
   (1) Nitroethane; C2H5NO2; [79-24-3]  NIST Chemistry WebBook for detail
   (2) Water; H2O; [7732-18-5]  NIST Chemistry WebBook for detail
Original Measurements:
   Zhuravleva, I.K.; Zhuravlev, E.F.; Khotkovskaya, T.L., Zh. Prikl. Khim. (Leningrad) 49, 2586 (1976); Deposited Doc., VINITI 1951 (1976).

 Variables:
   Temperature = 295 K to 444 K

 Prepared By:
   V. P. Sazonov and N. I. Lisov

 Experimental Data:   (Notes on the Nomenclature)
  
Mutual solubility of nitroethane (1) and water (2)
t/°CT/K102 * Mass Fraction w1Mole Fraction x1 (compiler)Comment(s)
22.0295.2--water-rich phase
30.0303.2 4.50.011water-rich phase
41.0314.2--water-rich phase
50.0323.2 5.50.014water-rich phase
55.0328.2--water-rich phase
62.0335.2 6.40.016water-rich phase
64.0337.2--water-rich phase
71.0344.2 7.00.018water-rich phase
80.0353.2--water-rich phase
135.0408.220.00.057water-rich phase
150.0423.2--water-rich phase
159.0432.2--water-rich phase
160.0433.235.00.114water-rich phase
164.0437.2--water-rich phase
167.5440.745.00.164water-rich phase
168.0441.2--water-rich phase
169.0442.2--water-rich phase
169.5442.750.00.194water-rich phase
170.5443.755.00.227water-rich phase
170.5443.755.00.227water-rich phase
Mutual solubility of nitroethane (1) and water (2)
t/°CT/K102 * Mass Fraction w1Mole Fraction x1 (compiler)Comment(s)
22.0295.299.20.967nitroethane-rich phase
30.0303.298.90.956nitroethane-rich phase
41.0314.298.60.944nitroethane-rich phase
50.0323.2--nitroethane-rich phase
55.0328.298.00.922nitroethane-rich phase
62.0335.2--nitroethane-rich phase
64.0337.297.80.914nitroethane-rich phase
71.0344.2--nitroethane-rich phase
80.0353.296.00.852nitroethane-rich phase
135.0408.2--nitroethane-rich phase
150.0423.280.70.501nitroethane-rich phase
159.0432.277.00.446nitroethane-rich phase
160.0433.2--nitroethane-rich phase
164.0437.270.00.359nitroethane-rich phase
167.5440.7--nitroethane-rich phase
168.0441.267.50.333nitroethane-rich phase
169.0442.260.00.263nitroethane-rich phase
169.5442.7--nitroethane-rich phase
170.5443.7--nitroethane-rich phase
170.5443.755.00.227 (UCST)nitroethane-rich phase
 Method/Apparatus/Procedure:
   The synthetic method1 was used. No details were reported.

 Source and Purity of Materials:
   (1) Source not specified; purity not specified; distilled; n(20°C,D) = 1.3905, d(20°C, 4°C) = 1.0525.
   (2) Distilled; n(25°C,D) = 1.333.

 Estimated Errors:
   Solubility: Not reported.
   Temperature: Not reported.

 References:
   1 V. F. Alekseev, Zh. Russ. Fiz.-Khim. O-va 8, 249 (1876).