IUPAC-NIST Solubility Database
NIST Standard Reference Database 106


Glass Ball as Bullet Solubility System: Nitroethane with Dodecanoic acid

Components:
   (1) Dodecanoic acid; C12H24O2; [143-07-7]  NIST Chemistry WebBook for detail
   (2) Nitroethane; C2H5NO2; [79-24-3]  NIST Chemistry WebBook for detail

Original Measurements:
   Hoerr, C.W.; Ralston, A.W., J. Org. Chem. 9, 329-37 (1944).

Variables:
   Temperature = 273 K to 313 K

Prepared By:
   N. I. Lisov and V. P. Sazonov

Experimental Data:   (Notes on the Nomenclature)
  
Solubility of dodecanoic acid (2) in nitroethane (1)
t/°CT/K102 * Mass Fraction w2 (compiler)g2/g1Mole Fraction x2 (compiler)
0.0273.2 1.8 1.9 x 1020.007
10.0283.2 2.7 2.8 x 1020.010
20.0293.2 5.1 5.4 x 1020.020
30.0303.214.0 16.3 x 1020.058
40.0313.293.61460 x 1020.846
Method/Apparatus/Procedure:
   The synthetic method, as described in Hoerr et al.1 was used. No details were reported.

Source and Purity of Materials:
   (1) Source not specified; purified according to Hoerr et al.1 (dried and twice distilled).
   (2) Source not specified; purified according to Pool and Ralston,2 f. p. = 43.92 °C.

Estimated Errors:
   Solubility: Not specified.
   Temperature: Not specified.

References:
   1 C. W. Hoerr, E. F. Binkerd, W. O. Pool, and A. W. Ralston, J. Org. Chem. 9, 68 (1944).
   2 W. O. Pool and A. W. Ralston, Ind. Eng. Chem. 34, 1104 (1942).