IUPAC-NIST Solubility Database
NIST Standard Reference Database 106


Glass Ball as Bullet Solubility System: Decane with Water

Components:
   (1) Water; H2O; [7732-18-5]  NIST Chemistry WebBook for detail
   (2) Decane; C10H22; [124-18-5]  NIST Chemistry WebBook for detail

Original Measurements:
   Krasnoschchekova, R.Ya.; Gubergrits, M.Ya., Neftekhimiya 1973, 13, 885-8.

Variables:
   Temperature = 25 °C

Prepared By:
   A. Maczynski

Experimental Remarks:

   The solubility of decane in water at 25°C was reported to be x1 = 1.1 × 10–9.

The corresponding mass percent calculated by the compiler is 8.7 × 10–7 g(1)/100 g sln.

Experimental Data:   (Notes on the Nomenclature)
   Method/Apparatus/Procedure:
   A mixture of 10 mL and 300 mL (2) was placed in a double-walled bottom-stoppered vessel and vigouously stirred magnetically for 10-12 hr. The phases were allowed to separate; a first sample of the water phase was rejected and next 200 mL of this phase was taken, 20-mL aliquots were introduced into 40-mL hermetic bottles and (1) was allowed to equilibrate with the air, and the (1)-saturated air was analyzed by glc.

Source and Purity of Materials:
   (1) source not specified; CP reagent; purity not specified.
   (2) distilled.

Estimated Errors:

   Temperature: not specified.