IUPAC-NIST Solubility Database
NIST Standard Reference Database 106

Glass Ball as Bullet Solubility System: Fluorene with Aniline
Components:
   (1) Fluorene; C13H10; [86-73-7]  NIST Chemistry WebBook for detail
   (2) Aniline; C6H7N; [62-53-3]  NIST Chemistry WebBook for detail
Original Measurements:
   Mortimer, F.S., J. Am. Chem. Soc. 1923, 45, 633-641.

 Variables:
   Temperature = Temperature

 Prepared By:
   W.E. Acree, Jr.

 Experimental Data:   (Notes on the Nomenclature)
  
T/KMole Fraction x1Mole Fraction x2
2730.0240.976
2930.0560.944
3130.1170.883
3330.2320.768
3530.4270.573
 Method/Apparatus/Procedure:
   Experimental procedure not given in the reference. Compiler speculates that the experimental values were, in all likelihood, determined by a gravimetric method, which was common practice during this era. The method probably involved equilibrating excess solute and solvent in sealed containers, transfer of weighed aliquots of saturated solution to tared containers, evaporation of solvent, and weighing of solid residue  that remained.

 Source and Purity of Materials:
   (1) Purity and chemical source not given. Paper states only that the solute was carefully purified.
   (2) Purity and chemical source not given. Paper states only that the solvent was carefully purified.

 Estimated Errors:

   Temperature: T/K: ± 2 (compiler). x1: ± 8 % (relative error, by compiler).