IUPAC-NIST Solubility Database
NIST Standard Reference Database 106


Glass Ball as Bullet Solubility System: Calcium formate with Water

Components:
   (1) Calcium formate; Ca(CHO2)2; [544-17-2]  NIST Chemistry WebBook for detail
   (2) Water; H2O; [7732-18-5]  NIST Chemistry WebBook for detail

Original Measurements:
   Krasnitzki, E. R.,Monatsh. Chem. 8, 595 (1887).

Variables:
   Temperature = 0.8 ºC to 80.5 ºC.

Prepared By:
   Chr.Balarew

Experimental Remarks:

   The molality values were calculated by the compilers.
Authors' Comment: The solubility data (g/100g H2O) are the mean values obtained by the cooling and by the heating method.

Experimental Data:   (Notes on the Nomenclature)
(Please see footnotes following the table(s).)
  
Solubility of calcium formate in water
t/°Cg1/g2PhaseMass Fraction w1m1 [mol kg-1]Solid Phase(s)a
0.816.28Liquid14.001.251A
15.516.72Liquid14.321.284A
26.317.04Liquid14.551.309A
39.717.36Liquid14.791.334A
56.617.70Liquid15.031.359A
76.017.99Liquid15.241.382A
80.518.07Liquid15.301.388A
Notes:
   a  The solid phase is: A = Ca(CHO2)2.

Method/Apparatus/Procedure:
   The apparatus and method were described earlier.1 The mixtures were shaken for 1-1.5 h. Dilute sulfuric acid was added to a weighed sample. The mixture was evaporated on a water bath. The remaining sulfuric acid was driven off by heating to constant weight of calcium sulfate.

Source and Purity of Materials:
   Calcium carbonate, obtained by heating calcium oxalate, was dissolved in formic acid. The crystals were recrystallized and analyzed.

Estimated Errors:
   Solubility: ± 0.04 g/100 g water.

References:
   1Raupenstrauch, Monatsh. Chem. 6, 563 (1885).